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Book Cover
Book
Author Nelson, John H. (John Henry), 1940-

Title Nuclear magnetic resonance spectroscopy / John H. Nelson
Published Upper Saddle River, NJ : Prentice Hall/Pearson Education, 2003 [that is, 2002]

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Location Call no. Vol. Availability
 W'PONDS  543.0877 Nel/Nmr  AVAILABLE
Description 464 pages : illustrations
Contents Physical and Chemical Constants -- Ch. 1. Basic Theory of NMR Spectroscopy -- 1.1. Nuclear Spin -- 1.2. Interaction of Nuclear Spins with Magnetic Fields -- 1.3. Precession and the Larmor Frequency -- 1.4. Nuclear Energy Levels and Relaxation -- 1.5. The Rotating Frame of Reference -- 1.6. The Bloch Equations -- Ch. 2. Measurement of the Spectrum: Instrumentation -- 2.1. Fundamental Components of an NMR Spectrometer -- 2.2. The Magnet -- 2.3. The Transmitter Coil -- 2.4. The Receiver Coil -- 2.5. The Sample -- 2.6. Obtaining a Spectrum -- 2.7. Continuous-Wave Experiments -- 2.8. Fourier Transform Experiments -- 2.9. Detecting the Signal and Digitizing the Data -- 2.10. Processing the Signal -- 2.11. The Fourier Transformation Process -- 2.12. Double and Triple Resonance -- 2.13. Homonuclear Decoupling -- 2.14. Heteronuclear Decoupling -- 2.15. Pulse Sequences -- 2.16. Signal-to-Noise Ratio -- Ch. 3. The Chemical Shift and Examples for Selected Nuclei -- 3.1. General Considerations -- 3.2. Proton Chemical Shifts -- 3.3. Carbon Chemical Shifts -- 3.4. Boron Chemical Shifts -- 3.5. Nitrogen Chemical Shifts -- 3.6. Flourine Chemical Shifts -- 3.7. Phosphorus Chemical Shifts -- 3.8. Platinum Chemical Shifts -- Ch. 4. Symmetry and NMR Spectroscopy -- 4.1. Introduction -- 4.2. Spin-System Designation -- Ch. 5. Spin-Spin Coupling and NMR Spin Systems -- 5.1. General Considerations -- 5.2. Quantum Mechanics and NMR Spectroscopy -- Ch. 6. Typical Magnitudes of Selected Coupling Constants -- 6.1. General Considerations -- 6.2. Vicinal ([superscript 3]J[subscript HH]) Couplings -- 6.3. Geminal ([superscript 2]J[subscript HH]) Couplings -- 6.4. Long-range H - H Couplings -- 6.5. [superscript 1]J[subscript CH] Couplings -- 6.6. [superscript 2]J[subscript CH] and [superscript 3]J[subscript CH] Couplings -- 6.7. [superscript n]J[subscript CC] Couplings -- 6.8. [superscript n]J[subscript NH] and [superscript n]J[subscript NC] Couplings -- 6.9. [superscript n]J[subscript FX] Couplings -- 6.10. [superscript n]J[subscript PX] Couplings -- Ch. 7. Nuclear Spin Relaxation -- 7.1. Introduction -- 7.2. Different Types of Relaxation -- 7.3. Microscopic Origin of Relaxation -- 7.4. Different Types of Relaxation Mechanisms -- 7.5. Experimental Behavior of Nuclear Relaxation -- 7.6. Experimental Measurement of Relaxation Times -- 7.7. The [superscript 13]C Nucleus and Its Dominant Relaxation Mechanisms -- Ch. 8. The Nuclear Overhauser Effect -- 8.1. Introduction -- 8.2. Experimental Measurement -- Ch. 9. Editing [superscript 13C] NMR Spectra -- 9.1. Introduction -- 9.2. Attached-Proton Test (APT) -- 9.3. Distortionless Enhancement by Polarization Transfer (DEPT) -- Ch. 10. Two-Dimensional NMR Spectroscopy -- 10.1. Introduction -- 10.2. The Basic Two-Dimensional NMR Experiment -- 10.3. Graphical Presentation of 2D NMR Spectra -- 10.4. Two-Dimensional J-Resolved Spectroscopy -- 10.5. Two-Dimensional Correlated Spectroscopy -- 10.6. Two-Dimensional Exchange Spectroscopy (NOESY and EXSY) -- 10.7. The Two-Dimensional INADEQUATE Experiment -- 10.8. HMQC and HMBC Spectra -- 10.9. Data Acquisition and Processing Parameters in 2D NMR Spectroscopy -- Ch. 11. Dynamic NMR Spectroscopy -- 11.1. Introduction -- 11.2. Determination of Exchange Rates -- 11.3. Coalescence Temperatures and Rate Constants at Coalescence -- 11.4. Complete Line-Shape Analysis -- 11.5. Activation Parameters -- 11.6. Equilibrium Thermodynamics -- 11.7. Examples of Dynamic Processes Studied by NMR Spectroscopy -- Ch. 12. Lanthanide-Shift Reagents -- 12.1. Introduction -- 12.2. Theory of Shift Reagent-Substrate Interaction -- 12.3. Contact and Dipolar Interactions -- 12.4. Determination of Molecular Geometry -- 12.5. Chiral Lanthanide-Shift Reagents -- 12.6. Practical Considerations -- Ch. 13. NMR of Solids -- 13.1. Introduction -- 13.2. Proton Dipolar Broadening -- 13.3. Chemical-Shift Anisotropy -- 13.4. Magic-Angles Spinning -- 13.5. Cross Polarization -- 13.6. Recapitulation -- 13.7. Crystallographic Equivalence, Chemical-Shift Equivalence, and Magnetic Equivalence in CP/MAS NMR Spectra -- 13.8. Molecular Motion in the Solid State -- Ch. 14. Problems -- Selected Values of Longitudinal Relaxation Times for Some Nuclei
Notes "Copyright c2003"
Bibliography Includes bibliographical references and index
Subject Nuclear magnetic resonance spectroscopy.
LC no. 00069869
ISBN 0130334510 alkaline paper