| Description |
1 online resource : text file, PDF |
| Series |
Food Analysis & Properties |
| Contents |
Cover -- Half Title -- Title Page -- Copyright Page -- Table of Contents -- Foreword -- Editors -- Contributors -- Section I : Regulatory Issues -- Chapter 1: European Union Monitoring Programs -- 1.1 Legal Frame -- 1.1.1 Regulation (EC) No. 882/2004 -- 1.1.2 Regulation (EC) No. 396/2005 -- 1.1.3 Regulation (EC) No. 178/2002 -- 1.2 Official Controls -- 1.2.1 EU-Coordinated Multiannual Control Program (EUCP) -- 1.2.2 National Control Programs for Pesticide Residues -- 1.3 Sampling Procedures -- 1.4 Official Laboratories |
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1.5 Annual Report 1.6 Overall -- References -- Chapter 2: Monitoring Programs in the United States -- 2.1 Introduction -- 2.2 Laws, Regulations, and Roles of U.S. Agencies -- 2.3 U.S. Pesticide Monitoring Programs -- 2.3.1 USFDA Pesticide Programs -- 2.3.1.1 USFDA Regulatory Pesticide Monitoring Program -- 2.3.1.2 USFDA TDS -- 2.3.2 USDA Pesticide Programs -- 2.3.2.1 USDA NRP -- 2.3.2.2 USDA PDP -- 2.4 Summary -- References -- Section II : Sample Preparation -- Chapter 3: Most Common Sample Preparation Methods for Pesticide Residue Analysis |
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3.1 Introduction 3.2 Luke Method -- 3.2.1 New Dutch Mini-Luke (NL-Method) -- 3.3 EtAc Method -- 3.3.1 History -- 3.3.2 Analytical Procedure and Critical Parameters -- 3.3.2.1 Type of Matrices and Sample Amount -- 3.3.2.2 Extraction Strategies -- 3.3.2.3 Instrumentation -- 3.4 EtAc Method vs. Mini-Luke and QuEChERS -- 3.5 MSPD -- 3.5.1 Introduction -- 3.5.2 Analytical Procedure -- 3.5.2.1 Sample Blending Step -- 3.5.2.2 Packing of SPE Column -- 3.5.2.3 Elution of Analytes -- 3.5.3 Critical Parameters |
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3.5.3.1 Solid Support and Bonded Phase Used 3.5.3.2 Nature and Homogeneity of the Sample Matrix -- 3.5.3.3 Sample to Solid Support Ratio -- 3.5.3.4 Elution Volume, Rate, and Solvent Elution Sequence Performed -- 3.5.3.5 Use of Matrix Modifiers -- 3.5.3.6 Blending Process -- 3.5.4 Applications -- 3.6 Conclusions -- References -- Chapter 4: Sample Preparation Methods for the Determination of Organic Micropollutants -- 4.1 General Introduction -- 4.2 Sample Preparation Methods Applied to Solid and Complex Samples -- 4.2.1 Ultrasonic-Assisted Extraction |
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4.2.2 Microwave-Assisted Extraction 4.2.3 Pressurized Liquid Extraction -- 4.2.4 Pressurized Hot Water Extraction -- 4.2.5 Supercritical Fluid Extraction -- 4.2.6 Solid-Phase Extraction -- 4.2.7 Solid-Phase Microextraction -- 4.2.8 Stir Bar Sorptive Extraction -- 4.2.9 Immuno-Affinity Extraction -- 4.2.10 Cloud-Point Extraction -- 4.2.11 Soxhlet Extraction -- 4.3 Conclusions -- References -- Chapter 5: QuEChERS and Other MRM Sample Preparation Methods -- 5.1 Introduction -- 5.2 Solid Phase Micro Extraction |
| Summary |
"Pesticide residues can persist for some time and can be harmful to human health, wildlife and the global environment. Determination of such residues helps to keep the production sustainability and to design policies to protect endangered ecosystems. This book presents the key features of pesticide residues analysis in food matrices. It provides both theoretical and practical, updated information on instrumental advances and their applications as well as the main trends in sample preparations protocols employed in MRM pesticide residue analysis."--Provided by publisher |
| Bibliography |
Includes bibliographical references and index |
| Notes |
Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force. WlAbNL |
| Subject |
Pesticide residues in food.
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Food contamination.
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Food -- Analysis.
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Food Contamination
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Food Analysis
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TECHNOLOGY & ENGINEERING -- Food Science.
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BUSINESS & ECONOMICS -- Infrastructure.
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SOCIAL SCIENCE -- General.
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Food -- Analysis
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Food contamination
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Pesticide residues in food
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| Form |
Electronic book
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| Author |
Nollet, Leo M. L
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Fernandez-Alba, Amadeo R
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| ISBN |
9781315118352 |
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1315118351 |
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9781482235098 |
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1482235099 |
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9781351644631 |
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1351644637 |
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