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Book Cover
E-book
Author Kissinger, Peter

Title Laboratory Techniques in Electroanalytical Chemistry, Revised and Expanded
Edition 2nd ed
Published Boca Raton : Chapman and Hall/CRC, 2018

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Description 1 online resource (910 pages)
Contents Cover; Half Title; Title Page; Copyright Page; Table of Contents; Preface; Contributors; 1 An Overview; I. Some Philosophy; II. Progress and Prognosis; III. So Much Nomenclature, So Much Jargon; Bibliography; 2 Fundamental Concepts of Analytical Electrochemistry; I. Introduction; II. Mass Transport: Linear Diffusion; III. The Charged Interphase; IV. The Nernst Equation and Electrochemical Reversibility; V. Coupled Chemical Reactions and Chemical Reversibility; VI. Liquid-Solid Adsorption; VII. Conclusion; References; 3 Large-Amplitude Controlled-Potential Techniques; I. Introduction
II. Potential-Step Techniques in Stationary SolutionIII. Potential-Scan Techniques in Stationary Solution; IV. Controlled-Potential Techniques in Flowing Solution; References; 4 Large-Amplitude Controlled-Current Techniques; I. Controlled-Current Techniques in Stationary Solution; II. Controlled-Current Techniques in Flowing Solution; References; 5 Small-Amplitude Controlled-Potential Techniques; I. Introduction; II. Faradaic Impedance; III. Sinusoidal Alternating-Current Voltammetry; IV. Cyclic Alternating-Current Voltammetry; V. Tensammetry; VI. Step-Based Methods
VII. Staircase VoltammetryVIII. Differential Pulse Methods; IX. Square-Wave Methods; X. Differential "Normal Pulse" Voltammetry; XI. Conclusion; References; 6 Introduction to Analog Instrumentation; I. Classical Controlled-Potential Instrumentation; II. Controlled-Potential Instrumentation Based on Operational Amplifiers; III. Classical Controlled-Current Instrumentation; IV. Controlled-Current Instrumentation Based on Operational Amplifiers; V. Microprocessor-Based Electrochemical Instrumentation; VI. Conclusion; Reference
7 Overcoming Solution Resistance with Stability and Grace in Potentiostatic CircuitsI. Introduction; II. Input-Output Relations of Cells and Potentiostats; III. Stability of Potentiostat-Cell Circuits and the Role of Ru; IV. Compensation for iRu by Positive Feedback; V. Achieving Stability Through Gain-Frequency Shaping; VI. Real Systems; Appendix; Bibliography; 8 Conductivity and Conductometry; I. Some Basic Relationships; II. DC Contact Measurement of Conductance; III. Capacitive Contact Measurement of Conductance; References; 9 Electrochemical Cells; I. Design Concepts
II. Stationary-Solution ExperimentsIII. Convected-Solution Experiments; IV. Thin-Layer Cell Design; V. Cells for Spectroelectrochemistry; References; 10 Carbon Electrodes; I. Introduction; II. Performance Criteria; III. Carbon Electrode Materials Properties; IV. Common Carbon Electrode Materials; V. Selection of Carbon Electrodes for Analytical Applications; References; 11 Film Electrodes; I. Introduction; II. Applications of Thin-Film Electrodes; III. Properties of Film Electrodes; IV. Metal Film Electrodes; V. Carbon Film Electrodes; VI. Semiconductor Film Electrodes
Notes VII. Techniques of Cell Design Based on Film Electrodes
Print version record
Form Electronic book
Author Heineman, William R
ISBN 9781351990714
1351990713