| Description |
1 online resource (xx, 449 pages) |
| Series |
EMagRes books |
|
eMagRes books.
|
| Contents |
The discovery and demonstration of dynamic nuclear polarization : a personal and historical account / Charles P. Slichter -- DNP mechanisms / Krishnendu Kundu, Frédéric Mentink-Vigier, Akiva Feintuch, and Shimon Vega -- Pulsed dynamic nuclear polarization / Kong Ooi Tan, Sudheer Jawla, Richard J. Temkin, and Robert G. Griffin -- MAS-DNP enhancements : hyperpolarization, depolarization, and absolute sensitivity / Sabine Hediger, Daniel Lee, Frédéric Mentink-Vigier, and Gaël De Paëpe -- Polarizing agents : evolution and outlook in free radical development for DNP / Gilles Casano, Hakim Karoui, and Olivier Ouari -- Paramagnetic metal ions for dynamic nuclear polarization / Björn Corzilius -- Instrumentation for high-field dynamic nuclear polarization NMR spectroscopy / Guy M. Bernard and Vladimir K. Michaelis -- Millimeter-wave sources for DNP-NMR / Monica Blank and Kevin L. Felch -- Cryogenic platforms and optimized DNP sensitivity / Yoh Matsuki and Toshimichi Fujiwara -- Versatile dynamic nuclear polarization hardware with integrated electron paramagnetic resonance capabilities / Alisa Leavesley, Ilia Kaminker, and Songi Han -- Dissolution dynamic nuclear polarization methodology and instrumentation / Dennis Kurzbach and Sami Jannin -- Introduction to dissolution DNP : overview, instrumentation, and human applications / Jan H. Ardenkjaer-Larsen -- Liquid-state Overhauser DNP at high magnetic fields / Vasyl P. Denysenkov and Thomas F. Prisner -- Overhauser DNP in liquids on 13C nuclei / Marina Bennati and Tomas Orlando -- DNP and cellular solid-state NMR / Alessandra Lucini Paioni, Marie A.M. Renault, and Marc Baldus -- Cryo-trapped intermediates of retinal proteins studied by DNP-enhanced MAS NMR spectroscopy / Johanna Becker-Baldus and Clemens Glaubitz -- DNP solid-state NMR of biological membranes / Burkhard Bechinger -- DNP in materials science : touching the surface / Pierrick Berruyer, Lyndon Emsley, and Anne Lesage -- Growing signals from the noise : challenging nuclei in materials DNP / Frédéric A. Perras, Takeshi Kobayashi, and Marek Pruski -- DNP-enhanced solid-state NMR spectroscopy of active pharmaceutical ingredients / Li Zhao, Arthur C. Pinon, Lyndon Emsley, and Aaron J. Rossini -- In vivo hyperpolarized 13C MRS and MRI applications / Irene Marco-Rius and Arnaud Comment -- Dissolution dynamic nuclear polarization / Walter Köckenberger |
| Summary |
This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization—from long-proven, early developments, up to today’s hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined. Handbook of High Field Dynamic Nuclear Polarization is presented in three sections—Theoretical Aspects, DNP Development (instrumentation / radical / sample), and DNP NMR Applications. The first section offers chapters on; solid and cross effect DNP; thermal mixing; Overhauser; and dissolution DNP. The second looks at: microwave technology, gyrotron, and IOE; homebuilt and commercial DNP spectrometers; and glassing vs. solvent-free DNP. The final section provides information on; amyloid, membrane, and nanocrystalline proteins; metals, and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more |
| Bibliography |
Includes bibliographical references and index |
| Notes |
Online resource; title from digital title page (viewed on March 17, 2020) |
| Subject |
Polarization (Nuclear physics)
|
|
Nuclear magnetic resonance spectroscopy.
|
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Nuclear magnetic resonance spectroscopy
|
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Polarization (Nuclear physics)
|
| Form |
Electronic book
|
| Author |
Michaelis, Vladimir K., editor.
|
|
Griffin, Robert G., editor.
|
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Corzilius, Björn (Professor of physical chemistry), editor.
|
|
Vega, Shimon, editor.
|
| LC no. |
2019052236 |
| ISBN |
1119441668 |
|
9781119441694 |
|
1119441692 |
|
9781119441663 |
|
