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Book Cover
E-book
Author Thomas, Robert

Title Practical Guide to ICP-MS and Other Atomic Spectroscopy Techniques A Tutorial for Beginners
Edition 4th ed
Published Milton : Taylor & Francis Group, 2023

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Description 1 online resource (461 p.)
Series Practical Spectroscopy Series
Practical spectroscopy.
Contents Cover -- Half Title -- Series -- Title -- Copyright -- Contents -- Foreword -- Preface -- Acknowledgments -- About the Author -- Chapter 1 An Overview of ICP Mass Spectrometry -- 1.1 Principles of Operation -- Chapter 2 Principles of Ion Formation -- 2.1 Ion Formation -- 2.2 Natural Isotopes -- Chapter 3 Sample Introduction -- 3.1 Aerosol Generation -- 3.2 Droplet Selection -- 3.3 Nebulizers -- 3.4 Concentric Design -- 3.5 Cross-Flow Design -- 3.6 Microflow Design -- 3.7 Spray Chambers -- 3.8 Double-Pass Spray Chamber -- 3.9 Cyclonic Spray Chamber -- 3.10 Aerosol Dilution
3.11 Final Thoughts -- Chapter 4 Plasma Source -- 4.1 The Plasma Torch -- 4.2 Formation of an ICP Discharge -- 4.3 The Function of the RF Generator -- 4.4 Ionization of the Sample -- Chapter 5 Interface Region -- 5.1 Capacitive Coupling -- 5.2 Ion Kinetic Energy -- 5.3 Benefits of a Well-Designed Interface -- 5.4 Final Thoughts -- Chapter 6 Ion-Focusing System -- 6.1 Role of the Ion Optics -- 6.2 Dynamics of Ion Flow -- 6.3 Commercial Ion Optic Designs -- Chapter 7 Mass Analyzers: Quadrupole Technology -- 7.1 Basic Principles of Operation -- 7.2 Quadrupole Performance Criteria -- 7.3 Resolution
7.4 Abundance Sensitivity -- 7.5 Benefit of Good Abundance Sensitivity -- Chapter 8 Mass Analyzers: Double-Focusing Magnetic Sector Technology -- 8.1 Magnetic-Sector Mass Spectroscopy: A Historical Perspective -- 8.2 Use of Magnetic-Sector Technology for ICP-MS -- 8.3 Principles of Operation of Magnetic-Sector Technology -- 8.4 Resolving Power -- 8.5 Other Benefits of Magnetic-Sector Instrumentation -- 8.6 Simultaneous-Measurement Approach Using One Detector -- 8.7 Final Thoughts -- Chapter 9 Mass Analyzers: Time-of-Flight Technology -- 9.1 Basic Principles of TOF Technology
9.2 Commercial Designs -- 9.3 Differences between Orthogonal and On-Axis TOF -- 9.4 Benefits of TOF Technology for ICP-MS -- 9.5 Rapid Transient Peak Analysis -- 9.6 Improved Precision -- 9.7 Rapid Data Acquisition -- 9.8 High-Speed Multi-Elemental Imaging Using Laser Ablation Coupled with TOF-ICP-MS -- 9.9 Laser Ablation Laser Ionization Time-of-Flight Mass Spectrometry -- 9.10 Final Thoughts -- Chapter 10 Mass Analyzers: Collision/Reaction Cell and Interface Technology -- 10.1 Basic Principles of Collision/Reaction Cells -- 10.2 Different Collision/Reaction Cell Approaches
10.3 Collisional Mechanisms Using Nonreactive Gases and Kinetic Energy Discrimination -- 10.4 Reaction Mechanisms with Highly Reactive Gases and Discrimination by Selective Bandpass Mass Filtering -- 10.5 Dynamic Reaction Cell -- 10.6 Low-Mass Cutoff Collision/Reaction Cell -- 10.7 Using Reaction Mechanisms in a Collision Cell -- 10.8 The Universal Cell -- 10.9 The Collision/Reaction Interface -- 10.10 Detection Limit Comparison of Single-Quadrupole CRC Systems -- 10.11 Triple-Quadrupole Systems -- 10.12 M/S Mode -- 10.13 MS/MS Mode -- 10.14 On-Mass MS/MS Mode -- 10.15 Mass-Shift MS/MS Mode
Notes Description based upon print version of record
10.16 Multi-Quad Systems
Form Electronic book
ISBN 9781000915471
1000915476