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Book Cover
E-book
Author Harwood, Laurence M

Title Experimental Organic Chemistry : Standard and Microscale
Edition 3rd ed
Published Somerset : John Wiley & Sons, Incorporated, 2017

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Description 1 online resource (690 pages)
Contents Title Page ; Copyright Page; Contents; About the authors; Preface to the third edition; About the companion website; Part 1 Laboratory practice ; Chapter 1 Safety in the chemical laboratory; 1.1 Essential rules for laboratory safety; 1.2 Hazardous chemicals; 1.3 Disposal of hazardous waste; 1.4 Accident procedures; Chapter 2 Glassware and equipment in the laboratory ; 2.1 Glass equipment; 2.2 Hardware; 2.3 Heating; 2.4 Stirring; 2.5 Vacuum pumps; 2.6 The rotary evaporator; 2.7 Catalytic hydrogenation; 2.8 Ozonolysis; 2.9 Irradiation; 2.10 Compressed gases
Chapter 3 Organic reactions: From starting materials to pure organic product 3.1 Handling chemicals; 3.2 The reaction; 3.3 Purification of organic compounds; Chapter 4 Qualitative analysis of organic compounds ; 4.1 Purity; 4.2 Determination of structure using chemical methods; Chapter 5 Spectroscopic analysis of organic compounds ; 5.1 Absorption spectroscopy; 5.2 Infrared spectroscopy; 5.3 Nuclear magnetic resonance spectroscopy; 5.4 Ultraviolet spectroscopy; 5.5 Mass spectrometry; Chapter 6 Keeping records: The laboratory notebook and chemical literature ; 6.1 The laboratory notebook
6.2 The research report6.3 The chemical literature; Part 2 Experimental procedures ; Introduction; List of experiments; Experiments that can be taken in sequence; Experiments that can be used to compare directly different techniques for undertaking a reaction; Experiments that illustrate particular techniques; Chapter 7 Functional group interconversions; 7.1 Simple transformations; 7.2 Reactions of alkenes; 7.3 Substitution; 7.4 Reduction; 7.5 Oxidation; 7.6 Rearrangements; Chapter 8 Carbon-carbon bond-forming reactions ; 8.1 Grignard and organolithium reagents; 8.2 Enolate anions
8.3 Heteroatom-stabilized carbanions 8.4 Aromatic electrophilic substitution; 8.5 Pericyclic reactions; 8.6 Metal-mediated coupling reactions ; Chapter 9 Experiments using enabling technologies; 9.1 Microwave chemistry; 9.2 Flow chemistry; Chapter 10 Projects; 10.1 Natural product isolation and identification; 10.2 Project in organic synthesis; 10.3 Aspects of physical organic chemistry; Appendices; Appendix 1 Organic solvents ; Appendix 2 Spectroscopic correlation tables ; Index of chemicals; General index; EULA
Notes Print version record
Subject Chemistry, Organic -- Laboratory manuals.
Chemistry, Organic
Genre/Form Laboratory manuals
Form Electronic book
Author Moody, Christopher J
ISBN 9781118683415
1118683412